Difficult to see iodine on the miniscus?

Chemistry discussion, revision, exam and homework help.

Announcements Posted on
Enter our travel-writing competition for the chance to win a Nikon 1 J3 camera 21-05-2013
IMPORTANT: You must wait until midnight (morning exams)/4.30AM (afternoon exams) to discuss Edexcel exams and until 1pm/6pm the following day for STEP and IB exams. Please read before posting, including for rules for practical and oral exams. 28-04-2013
Sign in to Reply
  1. BondCovalentBond's Avatar
    • New Member
    • Posts: 7
    Difficult to see iodine on the miniscus?
    Hi there,

    I'm using a 0.1 conc iodine and it's quite difficult to see where it is on the miniscus... any way I could make sure it's exactly on the miniscus? How would they do this in a real chemical industry?

    Many thanks !
  2. gemmaj's Avatar
    • Full Member
    • Posts: 119
    Re: Difficult to see iodine on the miniscus?
    this is in no way a really technical or accurate way of doing it but when we were using potassium manganate VII in a titration and we couldn't see the meniscus because the compound was quite a dark purple. Our teacher told us to shine a light through the burette (most of us used our phone screens) and this made it easier to distinguise where the meniscus was.

    There probably is a proper way to do it but this is what we used
  3. thelooby94's Avatar
    • Adored and Respected Member
    • Posts: 464
    Re: Difficult to see iodine on the miniscus?
    (Original post by gemmaj)
    this is in no way a really technical or accurate way of doing it but when we were using potassium manganate VII in a titration and we couldn't see the meniscus because the compound was quite a dark purple. Our teacher told us to shine a light through the burette (most of us used our phone screens) and this made it easier to distinguise where the meniscus was.

    There probably is a proper way to do it but this is what we used
    Sounds like you're doing my ISA

    Are you doing a year 13 ISA? Lol
  4. gemmaj's Avatar
    • Full Member
    • Posts: 119
    Re: Difficult to see iodine on the miniscus?
    (Original post by thelooby94)
    Sounds like you're doing my ISA

    Are you doing a year 13 ISA? Lol
    what's an ISA ? im in year 13 yeah but im on OCR is that different to your exam board ?
  5. thelooby94's Avatar
    • Adored and Respected Member
    • Posts: 464
    Re: Difficult to see iodine on the miniscus?
    (Original post by gemmaj)
    what's an ISA ? im in year 13 yeah but im on OCR is that different to your exam board ?
    It's Bsically an experiment and a follow up test

    In ours, we're doing a titration using potassium permanganate
  6. gemmaj's Avatar
    • Full Member
    • Posts: 119
    Re: Difficult to see iodine on the miniscus?
    (Original post by thelooby94)
    It's Bsically an experiment and a follow up test

    In ours, we're doing a titration using potassium permanganate
    oh ok! yeah we have those too we only did a normal practical with potassium permanganate though
  7. Crushy's Avatar
    • Benevolent Member
    • Location: UK
    • Posts: 826
    Re: Difficult to see iodine on the miniscus?
    I had this with 0.02 moldm-3 iodine. T'was pretty annoying at first but you get used to it. My teacher told me she had burettes with fluorescent increment markings at uni (that might answer your question on the industry solution), that'd make it so much easier...
Sign in to Reply
Share this discussion:  
Article updates
Moderators

We have a brilliant team of more than 60 volunteers looking after discussions on The Student Room, helping to make it a fun, safe and useful place to hang out.

Reputation gems:
The Reputation gems seen here indicate how well reputed the user is, red gem indicate negative reputation and green indicates a good rep.
Post rating score:
These scores show if a post has been positively or negatively rated by our members.