Hi,
In practical we did the reaction of iodolactonisation of 3-cyclohexene-carboxylic acid. So, C6H9CO2H + NaHCO3 + I2 + KI -----> C7H9IO2 (two possible products).
It can be controlled under kinetic or thermodynamic properties. In my case it forms a kinetic product (3,2,1)iodolactone (connecting carbons 2 and 3 on cycloxehane). All were mixed and stirred. Then, extracted with CHCl3 and further washed with Na2S2O3. Dried and evaporated.
Based on the lab expt., I don't know why I got really low yield (28%), though it should be high because under kinetic control it can't form the other possible product.
Please, please any suggestions on how to improve the yield and why is it low.
THANK YOU!